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TEM studies of 1 MeV Fe+ ion-irradiated W alloys by wet chemical method: high-temperature annealing and deuterium retention
Ding, Xiao-Yu1,2; Liu, Jia-Qin3,4; Luo, Lai-Ma3,4,5; Xu, Qiu6; Gao, Xiang7; Huang, Jian-Jun1; Yu, Bin2; Li, Jian-Gang1,7; Wu, Yu-Cheng3,4,5
2019
发表期刊NUCLEAR FUSION
ISSN0029-5515
通讯作者Wu, Yu-Cheng(ycwu@hfut.edu.cn)
摘要In this study, the microstructural changes in irradiated W-1 wt%Pr2O3, W-1 wt%La2O3, W-1 wt%TiC and W-1 wt%ZrC specimens by 1 MeV Fe+ ion irradiation to doses of 1 dpa at room temperature have been characterized by transmission electron microscopy (TEM) to understand the radiation damage. The specimens of 1 dpa were consecutively annealed at temperatures of 600 degrees C, 800 degrees C, 900 degrees C and 1100 degrees C for 1h, and the post-irradiation annealing effect on the microstructure was studied. Microstructural features such as dislocations, dislocation loops and dense dislocation networks were observed by the means of TEM. There was a significant change in the microstructure of the tungsten (W) after irradiation and post-irradiation annealing. W-1 wt%TiC likely consisted of fewer radiation-induced defects and hence exhibits higher resistance to radiation-induced microstructural changes than the others. The general trend is that the density of defect clusters decreases while the average size of the clusters increases with the annealing temperature. A complete removal of dislocation structures at 1100 degrees C occurred in all materials. The irradiation damage effect of Fe+ ions on the deuterium retention of as-synthesized W-based composites was investigated. Thermal desorption spectroscopy of W implanted with D-2 (-) ions was performed using the low-energy ion irradiation system of Kyoto University. Compared with the samples without Fe preirradiation, the deuterium retention of the four composites increased after Fe+ pre-irradiation. The retained amount of deuterium was also increased with the increase in the Fe+ irradiation dose. This is of vital importance to the scientific community working on these materials for extreme irradiating environments.
关键词tungsten ion irradiation microstructure evolution annealing effect TEM deuterium retention
DOI10.1088/1741-4326/aaeaee
关键词[WOS]DAMAGED TUNGSTEN ; SPARK PLASMA ; IN-SITU ; DOPED TUNGSTEN ; MICROSTRUCTURE ; NEUTRON ; NANOCRYSTALLINE ; COMPOSITES ; EVOLUTION ; BEHAVIOR
收录类别SCI
语种英语
资助项目Double First Class enhancing independent innovation and social service capabilities of Hefei University of Technology[4500-411104/011] ; Open Foundation of Key Laboratory of Advanced Functional Materials and Devices of the Anhui Province ; 111 Project[B18018] ; Fundamental Research Funds for the Central Universities[PA2018GDQT0010] ; National Natural Science Foundation of China[51474083] ; National Natural Science Foundation of China[51574101] ; National Magnetic Confinement Fusion Program[2014GB121001] ; National Magnetic Confinement Fusion Program[2014GB121001] ; National Natural Science Foundation of China[51574101] ; National Natural Science Foundation of China[51474083] ; Fundamental Research Funds for the Central Universities[PA2018GDQT0010] ; 111 Project[B18018] ; Open Foundation of Key Laboratory of Advanced Functional Materials and Devices of the Anhui Province ; Double First Class enhancing independent innovation and social service capabilities of Hefei University of Technology[4500-411104/011]
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WOS研究方向Physics
WOS类目Physics, Fluids & Plasmas
WOS记录号WOS:000450933100002
出版者IOP PUBLISHING LTD
引用统计
被引频次：5[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.hfcas.ac.cn:8080/handle/334002/34399
专题中科院等离子体物理研究所
通讯作者Wu, Yu-Cheng
作者单位1.Shenzhen Univ, Adv Energy Res Ctr, Shenzhen 518060, Peoples R China
2.Shenzhen Univ, Coll Optoelect Engn, Key Lab Optoelect Devices & Syst, Minist Educ & Guangdong Prov, Shenzhen 518060, Peoples R China
3.Key Lab Adv Funct Mat & Devices Anhui Prov, Hefei 230009, Anhui, Peoples R China
4.Base Introducing Talents Discipline Univ Adv Clea, Hefei 230009, Anhui, Peoples R China
5.Hefei Univ Technol, Sch Mat Sci & Engn, Hefei 230009, Anhui, Peoples R China
6.Kyoto Univ, Inst Integrated Radiat & Nucl Sci, Osaka Fu 5900494, Japan
7.Chinese Acad Sci, Inst Plasma Phys, Hefei 230031, Anhui, Peoples R China
推荐引用方式
GB/T 7714		 Ding, Xiao-Yu,Liu, Jia-Qin,Luo, Lai-Ma,et al. TEM studies of 1 MeV Fe+ ion-irradiated W alloys by wet chemical method: high-temperature annealing and deuterium retention[J]. NUCLEAR FUSION,2019,59(1):12.
APA Ding, Xiao-Yu.,Liu, Jia-Qin.,Luo, Lai-Ma.,Xu, Qiu.,Gao, Xiang.,...&Wu, Yu-Cheng.(2019).TEM studies of 1 MeV Fe+ ion-irradiated W alloys by wet chemical method: high-temperature annealing and deuterium retention.NUCLEAR FUSION,59(1),12.
MLA Ding, Xiao-Yu,et al."TEM studies of 1 MeV Fe+ ion-irradiated W alloys by wet chemical method: high-temperature annealing and deuterium retention".NUCLEAR FUSION 59.1(2019):12.
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